Collapse to view only § 471.31 - Effluent limitations representing the degree of effluent reduction attainable by the application of the best practicable control technology currently available (BPT).

§ 471.30 - Applicability; description of the nickel-cobalt forming subcategory.

This subpart applies to discharges of pollutants to waters of the United States, and introductions of pollutants into publicly owned treatment works from the process operations of the nickel-cobalt forming subcategory.

§ 471.31 - Effluent limitations representing the degree of effluent reduction attainable by the application of the best practicable control technology currently available (BPT).

Except as provided in 40 CFR 125.30-125.32, any existing point source sub-

ject to this subpart must achieve the following effluent limitations for the process operations representing the degree of effluent reduction attainable by the application of the best practicable control technology currently available (BPT):

(a) Rolling spent neat oils—subpart C—BPT. There shall be no discharge of process wastewater pollutants.

(b) Rolling spent emulsions.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt rolled with emulsions Chromium0.0750.031 Nickel0.3270.216 Fluoride10.14.49 Oil and grease3.42.04 TSS6.973.32 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(c) Rolling contact cooling water.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt rolled with water Chromium1.660.679 Nickel7.244.79 Fluoride22599.6 Oil and grease75.445.3 TSS15573.5 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(d) Tube Reducing Spent Lubricant—subpart C—BPT. (1) There shall be no discharge of process wastewater pollutants except as provided under paragraph (d)(2) of this section.

(2) Process wastewater pollutants may be discharged, with no allowance for any pollutants discharged, provided the facility owner or operator demonstrates, on the basis of analytical methods set forth in or approved pursuant to 40 CFR part 136, that the concentrations of nitrosamine compounds in the wastewater discharged from the tube reducing process do not exceed 0.050 mg/l of N-nitrosodimethylamine, 0.020 mg/l of N-nitrosodiphenylamine, and 0.020 mg/l of N-nitrosodi-n-propylamine.

(3) The demonstration required under paragraph (d)(2) of this section shall be made once per month until the demonstration has been made for all three nitrosamine compounds for six consecutive months, after which time the demonstration may be made once per quarter. If a sample is found to contain any of the foregoing nitrosamine compounds at concentrations greater than those specified in paragraph (d)(2) of this section, the actions described in paragraph (d)(4) of this section shall be taken, and the demonstration required under paragraph (d)(2) of this section shall be made once per month until it has been made for all three nitrosamine compounds for six consecutive months.

(4) If sampling results show that any of the foregoing nitrosamine compounds is present in the process wastewater at concentrations greater than those specified in paragraph (d)(2) of this section, the facility owner or operator shall ensure that, within thirty days of receiving written notification of the sampling results, there is no further discharge of tube reducing spent lubricant wastewater until the owner or operator:

(i) Performs a subsequent analysis which demonstrates that the concentrations of the foregoing nitrosamine compounds do not exceed the levels specified in paragraph (d)(2) of this section; or

(ii) Substitutes a new tube reducing lubricant and thereafter complies with the requirements of paragraph (d)(3) of this section; or

(iii) Determines the source of the pollutant whose concentration exceeded the level specified in paragraph (d)(2) of this section and demonstrates to the satisfaction of the NPDES issuing authority that such source has been eliminated.

(5) The concentration limits specified in paragraph (d)(2) of this section apply at the point of discharge from the tube reducing process. However, sampling after the tube reducing wastewater has been commingled with other wastewaters is permitted if:

(i) Any dilution caused by the other wastewaters is taken into account in determining the appropriate (i.e., lower) allowable discharge concentration; and

(ii) An analytical method of sufficient sensitivity is used to measure the levels of each of the foregoing nitrosamine compounds in the wastewaters being sampled.

(e) Drawing spent neat oils—subpart C—BPT. There shall be no discharge of process wastewater pollutants

(f) Drawing spent emulsions.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt drawn with emulsions Chromium0.0420.017 Nickel0.1830.121 Fluoride5.682.52 Oil and grease1.911.15 TSS3.911.86 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(g) Extrusion spent lubricants—subpart C—BPT. There shall be no discharge of process wastewater pollutants.

(h) Extrusion press or solution heat treatment contact cooling water.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt heat treated Chromium0.0370.015 Nickel0.1600.106 Fluoride4.952.20 Oil and grease1.670.999 TSS3.411.63 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(i) Extrusion press hydraulic fluid leakage.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt extruded Chromium0.1020.042 Nickel0.4460.295 Fluoride13.86.13 Oil and grease4.642.79 TSS9.514.53 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(j) Forging equipment cleaning wastewater.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt forged Chromium0.0180.007 Nickel0.0770.051 Fluoride2.381.06 Oil and grease0.8000.480 TSS1.6400.780 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(k) Forging contact cooling water.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of forged nickel-cobalt cooled with water Chromium0.2090.086 Nickel0.9100.602 Fluoride28.212.5 Oil and grease9.485.69 TSS19.59.25 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(l) Forging press hydraulic fluid leakage.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt forged Chromium0.0830.034 Nickel0.3590.238 Fluoride11.24.94 Oil and grease3.742.25 TSS7.673.65 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(m) Forging spent lubricants—subpart C—BPT. There shall be no discharge of process wastewater pollutants.

(n) Stationary casting contact cooling water.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt cast with stationary casting methods Chromium5.332.18 Nickel23.315.4 Fluoride720320 Oil and grease242145 TSS496236 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(o) Vacuum melting steam condensate—subpart C—BPT. There shall be no allowance for the discharge of process wastewater pollutants.

(p) Metal powder production atomization wastewater.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt metal powder atomized Chromium1.160.472 Nickel5.033.33 Fluoride15669.2 Oil and grease52.431.5 TSS10851.1 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(q) Annealing and solution heat treatment contact cooling water—subpart C—BPT. There shall be no allowance for the discharge of process wastewater pollutants.

(r) Wet air pollution control scrubber blowdown.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt formed Chromium0.3570.146 Nickel1.561.03 Fluoride48.221.4 Oil and grease16.29.72 TSS33.215.8 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(s) Surface treatment spent baths.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt surface treated Chromium0.4120.169 Nickel1.801.19 Fluoride55.724.7 Oil and grease18.711.2 TSS38.418.3 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(t) Surface treatment rinse.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt surface treated Chromium10.44.25 Nickel45.330.0 Fluoride1410623 Oil and grease472283 TSS968460 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(u) Alkaline cleaning spent baths.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt alkaline cleaned Chromium0.0151.52 Nickel16.210.7 Fluoride502223 Oil and grease169101 TSS346165 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(v) Alkaline cleaning rinse.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt alkaline cleaned Chromium1.030.420 Nickel4.482.96 Fluoride13961.5 Oil and grease46.628.0 TSS95.645.5 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(w) Molten salt rinse.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt treated with molten salt Chromium3.721.52 Nickel16.210.7 Fluoride502223 Oil and grease169101 TSS346165 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(x) Ammonia rinse.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt treated with ammonia solution Chromium0.0070.003 Nickel0.0290.019 Fluoride0.8810.391 Oil and grease0.2960.178 TSS0.6070.289 pH( 1)

1 Within the range of 7.5 to 10.0 at all times.

(y) Sawing or grinding spent emulsions.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt sawed or ground with emulsions Chromium0.0180.007 Nickel0.0760.050 Fluoride2.351.04 Oil and grease0.7880.473 TSS1.620.769 pH( 1)

1 Within the range of 7.5 to 10.0 at all times.

(z) Sawing or grinding rinse.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of sawed or ground nickel-cobalt rinsed Chromium0.7970.326 Nickel3.482.30 Fluoride10847.8 Oil and grease36.221.7 TSS74.235.3 pH( 1)

1 Within the range of 7.5 to 10.0 at all times.

(aa) Steam Cleaning Condensate.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt steam cleaned Chromium0.0130.006 Nickel0.0580.039 Fluoride1.790.795 Oil and grease0.6020.361 TSS1.240.587 pH( 1)

1 Within the range of 7.5 to 10.0 at all times.

(bb) Hydrostatic tube testing and ultrasonic testing wastewater—subpart C—BPT. There shall be no allowance for the discharge of process wastewater pollutants.

(cc) Degreasing spent solvents—subpart C—BPT. There shall be no discharge of process wastewater pollutants.

(dd) Dye penetrant testing wastewater.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt tested with dye penetrant method Chromium0.0940.039 Nickel0.4090.271 Fluoride12.75.63 Oil and grease4.262.56 TSS8.744.16 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(ee) Electrocoating rinse.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt electrocoated Chromium1.480.607 Nickel6.474.28 Fluoride20189.0 Oil and grease67.440.5 TSS13865.7 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(ff) Miscellaneous wastewater sources.

Subpart C—BPT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt formed Chromium0.1080.044 Nickel0.4730.313 Fluoride14.76.50 Oil and grease4.922.95 TSS10.14.80 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

[50 FR 34270, Aug. 23, 1985; 51 FR 2884, Jan. 22, 1986, as amended at 54 FR 11348, Mar. 17, 1989]

§ 471.32 - Effluent limitations representing the degree of effluent reduction attainable by the application of the best available technology economically achievable (BAT).

Except as provided in 40 CFR 125.30 through 125.32, any existing point source subject to this subpart must achieve the following effluent limitations representing the degree of effluent reduction attainable by the application of the best available technology economically achievable (BAT):

(a) Rolling spent neat oils—subpart C—BAT. There shall be no discharge of process wastewater pollutants.

(b) Rolling spent emulsions.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt rolled with emulsions Chromium0.0630.026 Nickel0.0940.063 Fluoride10.14.49

(c) Rolling contact cooling water.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt rolled with water Chromium0.0280.011 Nickel0.0420.028 Fluoride4.491.99

(d) Tube Reducing Spent Lubricant—subpart C—BAT. (1) There shall be no discharge of process wastewater pollutants except as provided under paragraph (d)(2) of this section.

(2) Process wastewater pollutants may be discharged, with no allowance for any pollutants discharged, provided the facility owner or operator demonstrates, on the basis of analytical methods set forth in or approved pursuant to 40 CFR part 136, that the concentrations of nitrosamine compounds in the wastewater discharged from the tube reducing process do not exceed 0.050 mg/l of N-nitrosodimethylamine, 0.020 mg/l of N-nitrosodiphenylamine, and 0.020 mg/l of N-nitrosodi-n-propylamine.

(3) The demonstration required under paragraph (d)(2) of this section shall be made once per month until the demonstration has been made for all three nitrosamine compounds for six consecutive months, after which time the demonstration may be made once per quarter. If a sample is found to contain any of the foregoing nitrosamine compounds at concentrations greater than those specified in subparagraph (d)(2) of this section, the actions described in paragraph (d)(4) of this section shall be taken, and the demonstration required under subparagraph (d)(2) of this section shall be made once per month until it has been made for all three nitrosamine compounds for six consecutive months.

(4) If sampling results show that any of the foregoing nitrosamine compounds is present in the process wastewater at concentrations greater than those specified in subparagraph (d)(2) of this section, the facility owner or operator shall ensure that, within thirty days of receiving written notification of the sampling results, there is no further discharge of tube reducing spent lubricant wastewater until the owner or operator:

(i) Performs a subsequent analysis which demonstrates that the concentrations of the foregoing nitrosamine compounds do not exceed the levels specified in paragraph (d)(2) of this section; or

(ii) Substitutes a new tube reducing lubricant and thereafter complies with the requirements of paragraph (d)(3) of this section; or

(iii) Determines the source of the pollutant whose concentration exceeded the level specified in paragraph (d)(2) of this section and demonstrates to the satisfaction of the NPDES issuing authority that such source has been eliminated.

(5) The concentration limits specified in paragraph (d)(2) of this section apply at the point of discharge from the tube reducing process. However, sampling after the tube reducing wastewater has been commingled with other wastewaters is permitted if:

(i) Any dilution caused by the other wastewaters is taken into account in determining the appropriate (i.e., lower) allowable discharge concentration; and

(ii) An analytical method of sufficient sensitivity is used to measure the levels of each of the foregoing nitrosamine compounds in the wastewaters being sampled.

(e) Drawing spent neat oils—subpart C—BAT. There shall be no discharge of process wastewater pollutants.

(f) Drawing spent emulsions.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt drawn with emulsions Chromium0.0360.015 Nickel0.0530.036 Fluoride5.682.52

(g) Extrusion spent lubricants—subpart C—BAT. There shall be no discharge of process wastewater pollutants.

(h) Extrusion press or solution heat treatment contact cooling water.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of extruded nickel-cobalt heat treated Chromium0.0310.013 Nickel0.0460.031 Fluoride4.952.20

(i) Extrusion press hydraulic fluid leakage.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt extruded Chromium0.0860.034 Nickel0.1280.086 Fluoride13.86.13

(j) Forging equipment cleaning wastewater.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt forged Chromium0.0020.0006 Nickel0.0020.002 Fluoride0.2380.106

(k) Forging contact cooling water.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of forged nickel-cobalt cooled with water Chromium0.0180.007 Nickel0.0260.018 Fluoride2.821.25

(l) Forging press hydraulic fluid leakage.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt forged Chromium0.0690.028 Nickel.1030.069 Fluoride11.24.94

(m) Forging spent lubricants—subpart C—BAT. There shall be no discharge of process wastewater pollutants.

(n) Stationary casting contact cooling water.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt cast with stationary casting methods Chromium0.4480.182 Nickel.666.448 Fluoride72.032.0

(o) Vacuum melting steam condensate—subpart C—BAT. There shall be no allowance for the discharge of wastewater pollutants.

(p) Metal powder production atomization wastewater.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt metal powder atomized Chromium0.9700.393 Nickel1.44.970 Fluoride15669.2

(q) Annealing and solution heat treatment contact cooling water—subpart C—BAT. There shall be no allowance for the discharge of wastewater pollutants.

(r) Wet air pollution control scrubber blowdown.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt formed Chromium0.3000.122 Nickel.446.300 Fluoride48.221.4

(s) Surface treatment spent baths.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt surface treated Chromium0.3460.141 Nickel.514.346 Fluoride55.724.7

(t) Surface treatment rinse.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt surface treated Chromium0.8730.354 Nickel1.30.873 Fluoride14162.3

(u) Alkaline cleaning spent baths.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt alkaline cleaned Chromium0.0130.005 Nickel0.0190.013 Fluoride2.020.895

(v) Alkaline cleaning rinse.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt alkaline cleaned Chromium0.0860.035 Nickel0.1280.086 Fluoride13.96.15

(w) Molten salt rinse.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly averge mg/off-kg (pounds per million off-pounds) of nickel-cobalt treated with molten salt Chromium0.3120.127 Nickel0.4640.312 Fluoride50.222.3

(x) Ammonia rinse.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt treated with ammonia solution Chromium0.0060.002 Nickel0.0080.006 Fluoride0.8810.391

(y) Sawing or grinding spent emulsions.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt sawed or ground with emulsions Chromium0.0150.006 Nickel0.0220.015 Fluoride2.351.04

(z) Sawing or grinding rinse.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of sawed or ground nickel-cobalt rinsed Chromium0.0670.027 Nickel0.1000.067 Fluoride10.84.78

(aa) Steam cleaning condensate.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt steam cleaned Chromium0.0110.005 Nickel0.0170.011 Fluoride1.790.795

(bb) Hydrostatic tube testing and ultrasonic testing wastewater—subpart C—BAT. There shall be no allowance for the discharge of process wastewater pollutants.

(cc) Degreasing spent solvents—subpart C—BAT. There shall be no discharge of process wastewater pollutants.

(dd) Dye penetrant testing wastewater.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt tested with dye penetrant method Chromium0.0790.032 Nickel0.1170.079 Fluoride12.75.63

(ee) Electrocoating rinse.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt electrocoated Chromium1.250.506 Nickel1.861.25 Fluoride20189.0

(ff) Miscellaneous wastewater sources.

Subpart C—BAT

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt formed Chromium0.0910.037 Nickel0.1360.091 Fluoride14.76.50
[50 FR 34270, Aug. 23, 1985; 51 FR 2885, Jan. 22, 1986, as amended at 54 FR 11348, Mar. 17, 1989; 54 FR 13606, Apr. 4, 1989]

§ 471.33 - New source performance standards (NSPS).

Any new source subject to this subpart must achieve the following new source performance standards (NSPS). The mass of pollutants in the nickel-cobalt forming process wastewater shall not exceed the following values:

(a) Rolling spent neat oils—subpart C—NSPS. There shall be no discharge of process wastewater pollutants.

(b) Rolling spent emulsions.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt rolled with emulsions Chromium0.0630.026 Nickel0.0940.063 Fluoride10.14.49 Oil and grease1.701.70 TSS2.552.04 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(c) Rolling contact cooling water.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt rolled with water Chromium0.0280.012 Nickel0.0420.028 Fluoride4.491.99 Oil and grease0.7540.754 TSS1.130.905 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(d) Tube Reducing Spent Lubricant—subpart C—NSPS. (1) There shall be no discharge of process wastewater pollutants except as provided under paragraph (d)(2) of this section.

(2) Process wastewater pollutants may be discharged, with no allowance for any pollutants discharged, provided the facility owner or operator demonstrates, on the basis of analytical methods set forth in or approved pursuant to 40 CFR part 136, that the concentrations of nitrosamine compounds in the wastewater discharged from the tube reducing process do not exceed 0.050mg/l of N-nitrosodimethylamine, 0.020 mg/l of N-nitrosodiphenylamine, and 0.020 mg/l of N-nitrosodi-n-propylamine.

(3) The demonstration required under paragraph (d)(2) of this section shall be made once per month until the demonstration has been made for all three nitrosamine compounds for six consecutive months, after which time the demonstration may be made once per quarter. If a sample is found to contain any of the foregoing nitrosamine compounds at concentrations greater than those specified in paragraph (d)(2) of this section, the actions described in paragraph (d)(4) of this section shall be taken, and the demonstration required under paragraph (d)(2) of this section shall be made once per month until it has been made for all three nitrosamine compounds for six consecutive months.

(4) If sampling results show that any of the foregoing nitrosamine compounds is present in the process wastewater at concentrations greater than those specified in paragraph (d)(2) of this section, the facility owner or operator shall ensure that, within thirty days of receiving written notification of the sampling results, there is no further discharge of tube reducing spent lubricant wastewater until the owner or operator:

(i) Performs a subsequent analysis which demonstrates that the concentrations of the foregoing nitrosamine compounds do not exceed the levels specified in paragraph (d)(2) of this section; or

(ii) Substitutes a new tube reducing lubricant and thereafter complies with the requirements of paragraph (d)(3) of this section; or

(iii) Determines the source of the pollutant whose concentration exceeded the level specified in paragraph (d)(2) of this section and demonstrates to the satisfaction of the NPDES issuing authority that such source has been eliminated.

(5) The concentration limits specified in paragraph (d)(2) of this section apply at the point of discharge from the tube reducing process. However, sampling after the tube reducing wastewater has been commingled with other wastewaters is permitted if:

(i) Any dilution caused by the other wastewaters is taken into account in determining the appropriate (i.e., lower) allowable discharge concentration; and

(ii) An analytical method of sufficient sensitivity is used to measure the levels of each of the foregoing nitrosamine compounds in the wastewaters being sampled.

(e) Drawing spent neat oils—subpart C—NSPS. There shall be no discharge of process wastewater pollutants.

(f) Drawing spent emulsions.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt drawn with emulsions Chromium0.0360.015 Nickel0.0530.036 Fluoride5.682.52 Oil and grease0.9540.954 TSS1.431.15 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(g) Extrusion spent lubricants—subpart C—NSPS. There shall be no discharge of process wastewater pollutants.

(h) Extrusion press or solution heat treatment contact cooling water.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of extruded nickel-cobalt heat treated Chromium0.0310.013 Nickel0.0460.031 Fluoride4.952.20 Oil and grease0.8320.832 TSS1.250.999 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(i) Extrusion press hydraulic fluid leakage.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt extruded Chromium0.0860.035 Nickel0.1280.086 Fluoride13.86.13 Oil and grease2.322.32 TSS3.482.79 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(j) Forging equipment cleaning wastewater.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt forged Chromium0.0020.00006 Nickel0.0020.002 Fluoride0.2380.106 Oil and grease0.0400.040 TSS0.0600.048 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(k) Forging contact cooling water.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of forged nickel-cobalt cooled with water Chromium0.0180.007 Nickel0.0260.018 Fluoride2.821.25 Oil and grease0.4740.474 TSS0.7110.569 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(l) Forging press hydraulic fluid leakage.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt forged Chromium0.0690.028 Nickel0.1030.069 Fluoride11.24.94 Oil and grease1.871.87 TSS2.812.25 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(m) Forging spent lubricants—subpart C—NSPS. There shall be no discharge of process wastewater pollutants.

(n) Stationary casting contact cooling water.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt cast with stationary casting methods Chromium0.4480.182 Nickel0.6660.448 Fluoride72.032.0 Oil and grease12.112.1 TSS18.214.5 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(o) Vacuum melting steam condensate—subpart C—NSPS. There shall be no allowance for the discharge of process wastewater pollutants.

(p) Metal powder production atomization wastewater.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt metal powder atomized Chromium0.9700.393 Nickel1.440.970 Fluoride15669.2 Oil and grease26.226.2 TSS39.331.5 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(q) Annealing and solution heat treatment contact cooling watersubpart C—NSPS. There shall be no allowance for the discharge of process wastewater pollutants.

(r) Wet air pollution control scrubber blowdown.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt formed Chromium0.3000.122 Nickel0.4500.300 Fluoride48.221.4 Oil and grease8.18.1 TSS12.29.72 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(s) Surface treatment spent baths.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt surface treated Chromium0.3460.141 Nickel0.5150.346 Fluoride55.724.7 Oil and grease9.359.35 TSS14.111.2 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(t) Surface treatment rinse.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt surface treated Chromium0.8740.354 Nickel1.300.873 Fluoride14162.3 Oil and grease23.623.6 TSS35.428.3 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(u) Alkaline cleaning spent baths.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt alkaline cleaned Chromium0.0130.005 Nickel0.0190.013 Fluoride2.020.895 Oil and grease0.3390.339 TSS0.5090.407 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(v) Alkaline cleaning rinse.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt alkaline cleaned Chromium0.0860.035 Nickel.128.086 Fluoride13.96.15 Oil and grease2.332.33 TSS3.502.80 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(w) Molten salt rinse.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt treated with molten salt Chromium0.3120.127 Nickel0.4640.312 Fluoride50.222.3 Oil and grease8.448.44 TSS12.710.1 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(x) Ammonia rinse.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt treated with ammonia solution Chromium0.0060.002 Nickel.008.006 Fluoride.881.391 Oil and grease.148.148 TSS222178 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(y) Sawing or grinding spent emulsions.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt sawed or ground Chromium0.0150.006 Nickel.002.015 Fluoride2.351.04 Oil and grease.394.394 TSS591473 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(z) Sawing or grinding rinse.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of sawed or ground nickel-cobalt rinsed Chromium0.0670.027 Nickel0.1000.067 Fluoride10.84.78 Oil and grease1.811.81 TSS2.72217 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(aa) Steam cleaning condensate.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt steam cleaned Chromium0.0110.005 Nickel0.0170.011 Fluoride1.790.795 Oil and grease0.3010.301 TSS0.4520.361 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(bb) Hydrostatic tube testing and ultrasonic testing wastewater—subpart C—NSPS. There shall be no discharge of process wastewater pollutants.

(cc) Degreasing spent solvents—subpart C—NSPS. There shall be no discharge of process wastewater pollutants.

(dd) Dye penetrant testing wastewater.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt tested with dye penetrant method Chromium0.0790.032 Nickel0.1170.079 Fluoride12.75.63 Oil and grease2.132.13 TSS3.202.56 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(ee) Electrocoating rinse.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt electrocoated Chromium1.250.506 Nickel1.861.25 Fluoride20189.0 Oil and grease33.733.7 TSS50.640.5 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

(ff) Miscellaneous wastewater sources.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt formed Chromium0.0910.037 Nickel0.1360.091 Fluoride14.76.50 Oil and grease2.462.46 TSS3.692.95 pH( 1)( 1)

1 Within the range of 7.5 to 10.0 at all times.

[50 FR 34270, Aug. 23, 1985; 51 FR 2885, Jan. 22, 1986, as amended at 54 FR 11349, Mar. 17, 1989; 54 FR 13606, Apr. 4, 1989]

§ 471.34 - Pretreatment standards for existing sources (PSES).

Except as provided in 40 CFR 403.7 and 403.13, any existing source subject to this subpart which introduces pollutants into a publicly owned treatment works must comply with 40 CFR part 403 and by August 23, 1988 achieve the following pretreatment standards for existing sources (PSES). The mass of wastewater pollutants in nickel-cobalt forming wastewater introduced into a POTW shall not exceed the following values:

(a) Rolling spent neat oils—subpart C—PSES. There shall be no discharge of process wastewater pollutants.

(b) Rolling spent emulsions.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt rolled with emulsions Chromium0.0630.026 Nickel0.0940.063 Fluoride10.14.49

(c) Rolling contact cooling water.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt rolled with water Chromium0.0280.011 Nickel0.0420.028 Fluoride4.491.99

(d) Tube Reducing Spent Lubricant—subpart C—PSES. (1) There shall be no discharge of process wastewater pollutants except as provided under paragraph (d)(2) of this section.

(2) Process wastewater pollutants may be discharged, with no allowance for any pollutants discharged, provided the facility owner or operator demonstrates, on the basis of analytical methods set forth in or approved pursuant to 40 CFR part 136, that the concentrations of nitrosamine compounds in the wastewater discharged from the tube reducing process do not exceed 0.050 mg/l of N-nitrosodimethylamine, 0.020 mg/l of N-nitrosodiphenylamine, and 0.020 mg/l of N-nitrosodi-n-propylamine.

(3) The demonstration required under paragraph (d)(2) of this section shall be made once per month until the demonstration has been made for all three nitrosamine compounds for six consecutive months, after which time the demonstration may be made once per quarter. If a sample is found to contain any of the foregoing nitrosamine compounds at concentrations greater than those specified in paragraph (d)(2) of this section, the actions described in paragraph (d)(4) of this section shall be taken, and the demonstration required under paragraph (d)(2) of this section shall be made once per month until it has been made for all three nitrosamine compounds for six consecutive months.

(4) If sampling results show that any of the foregoing nitrosamine compounds is present in the process wastewater at concentrations greater than those specified in paragraph (d)(2) of this section, the facility owner or operator shall ensure that, within thirty days of receiving written notification of the sampling results, there is no further discharge of tube reducing spent lubricant wastewater until the owner or operator:

(i) Performs a subsequent analysis which demonstrates that the concentrations of the foregoing nitrosamine compounds do not exceed the levels specified in paragraph (d)(2) of this section; or

(ii) Substitutes a new tube reducing lubricant and thereafter complies with the requirements of paragraph (d)(3) of this section; or

(iii) Determines the source of the pollutant whose concentration exceeded the level specified in paragraph (d)(2) of this section and demonstrates to the satisfaction of the POTW control authority that such source has been eliminated.

(5) The concentration limits specified in paragraph (d)(2) of this section apply at the point of discharge from the tube reducing process. However, sampling after the tube reducing wastewater has been commingled with other wastewaters is permitted if:

(i) Any dilution caused by the other wastewaters is taken into account in determining the appropriate (i.e., lower) allowable discharge concentration; and

(ii) An analytical method of sufficient sensitivity is used to measure the levels of each of the foregoing nitrosamine compounds in the wastewaters being sampled.

(e) Drawing spent neat oils—subpart C—PSES. There shall be no discharge of process wastewater pollutants.

(f) Drawing spent emulsions.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt drawn with emulsions Chromium0.0360.014 Nickel0.0530.036 Fluoride5.682.52

(g) Extrusion spent lubricants—subpart C—PSES. There shall be no discharge of process wastewater pollutants.

(h) Extrusion press or solution heat treatment contact cooling water.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of extruded nickel-cobalt heat treated Chromium0.0310.013 Nickel0.0460.031 Fluoride4.952.20

(i) Extrusion press hydraulic fluid leakage.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt extruded Chromium0.0860.034 Nickel0.1280.086 Fluoride13.86.13

(j) Forging equipment cleaning wastewater.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt forged Chromium0.0020.0006 Nickel0.0020.002 Fluoride0.2380.106

(k) Forging contact cooling water.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of forged nickel-cobalt cooled with water Chromium0.0180.007 Nickel0.0260.018 Fluoride2.821.25

(l) Forging press hydraulic fluid leakage.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt forged Chromium0.0690.028 Nickel0.1030.069 Fluoride11.24.94

(m) Forging spent lubricants—subpart C—PSES. There shall be no discharge of process wastewater pollutants.

(n) Stationary casting contact cooling water.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt cast with stationary methods Chromium0.4480.182 Nickel0.6660.448 Fluoride72.032.0

(o) Vacuum melting steam condensate—subpart C—PSES. There shall be no allowance for the discharge of wastewater pollutants.

(p) Metal powder production atomization wastewater.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt metal powder atomized Chromium0.9700.393 Nickel1.440.970 Fluoride15669.2

(q) Annealing and solution heat treatment contact cooling water—subpart C—PSES. There shall be no allowance for the discharge of wastewater pollutants.

(r) Wet air pollution control scrubber blowdown.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt formed Chromium0.3000.122 Nickel0.4460.300 Fluoride48.221.4

(s) Surface treatment spent baths.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt surface treated Chromium0.3460.141 Nickel0.5140.346 Fluoride55.724.7

(t) Surface treatment rinse.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt surface treated Chromium0.8730.354 Nickel1.300.873 Fluoride14162.3

(u) Alkaline cleaning spent baths.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt alkaline cleaned Chromium0.0130.005 Nickel0.0190.013 Fluoride2.020.895

(v) Alkaline cleaning rinse.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt alkaline cleaned Chromium0.0860.035 Nickel0.1280.086 Fluoride13.96.15

(w) Molten salt rinse.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt treated with molten salt Chromium0.3120.127 Nickel0.4640.312 Fluoride50.222.3

(x) Ammonia rinse.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt treated with ammonia solution Chromium0.0060.002 Nickel0.0080.006 Fluoride0.8810.391

(y) Sawing or grinding spent emulsions.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt sawed or ground with emulsions Chromium0.0150.006 Nickel0.0220.015 Fluoride2.351.04

(z) Sawing or grinding rinse.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of sawed or ground nickel-cobalt rinsed Chromium0.0670.027 Nickel0.1000.067 Fluoride10.84.78

(aa) Steam cleaning condensate.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt steam cleaned Chromium0.0110.005 Nickel0.0170.011 Fluoride1.790.795

(bb) Hydrostatic Tube Testing and Ultrasonic Testing Wastewater—subpart C—PSES. There shall be no allowance for the discharge of process wastewater pollutants.

(cc) Degreasing Spent Solvents—subpart C—PSES. There shall be no discharge of process wastewater pollutants.

(dd) Dye Penetrant Testing Wastewater.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt tested with dye penetrant method Chromium0.0790.032 Nickel0.1170.079 Fluoride12.75.63

(ee) Electrocoating rinse.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt electrocoated Chromium1.250.506 Nickel1.861.25 Fluoride20189.0

(ff) Miscellaneous wastewater sources.

Subpart C—PSES

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt formed Chromium0.0910.037 Nickel0.1360.091 Fluoride14.76.50
[50 FR 34270, Aug. 23, 1985; 51 FR 2885, Jan. 22, 1986, as amended at 54 FR 11349, Mar. 17, 1989; 54 FR 13606, Apr. 4, 1989]

§ 471.35 - Pretreatment standards for new sources (PSNS).

Except as provided in 40 CFR 403.7, any new source subject to this subpart which introduces pollutants into a publicly owned treatment works must comply with 40 CFR part 403 and achieve the following pretreatment standards for new sources. The mass of wastewater pollutants in nickel-cobalt forming process wastewater introduced into a POTW shall not exceed the following values:

(a) Rolling spent neat oils—subpart C—PSNS. There shall be no discharge of process wastewater pollutants.

(b) Rolling spent emulsions.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt rolled with emulsions Chromium0.0630.026 Nickel0.0940.063 Fluoride10.14.49

(c) Rolling contact cooling water.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt rolled with water Chromium0.0280.012 Nickel0.0420.028 Fluoride4.491.99

(d) Tube Reducing Spent Lubricant—subpart C—PSNS. (1) There shall be no discharge of process wastewater pollutants except as provided under paragraph (d)(2) of this section

(2) Process wastewater pollutants may be discharged, with no allowance for any pollutants discharged, provided the facility owner or operator demonstrates, on the basis of analytical methods set forth in or approved pursuant to 40 CFR part 136, that the concentrations of nitrosamine compounds in the wastewater discharged from the tube reducing process do not exceed 0.050 mg/l of N-nitrosodimethylamine, 0.020 mg/l of N-nitrosodiphenylamine, and 0.020 mg/l of N-nitrosodi-n-propylamine.

(3) The demonstration required under subparagraph (d)(2) of this section shall be made once per month until the demonstration has been made for all three nitrosamine compounds for six consecutive months, after which time the demonstration may be made once per quarter. If a sample is found to contain any of the foregoing nitrosamine compounds at concentrations greater than those specified in paragraph (d)(2) of this section, the actions described in paragraph (d)(4) of this section shall be taken, and the demonstration required under paragraph (d)(2) of this section shall be made once per month until it has been made for all three nitrosamine compounds for six consecutive months.

(4) If sampling results show that any of the foregoing nitrosamine compounds is present in the process wastewater at concentrations greater than those specified in subparagraph (d)(2) of this section, the facility owner or operator shall ensure that, within thirty days of receiving written notification of the sampling results, there is no further discharge of tube reducing spent lubricant wastewater until the owner or operator:

(i) Performs a subsequent analysis which demonstrates that the concentrations of the foregoing nitrosamine compounds do not exceed the levels specified in paragraph (d)(2) of this section (2); or

(ii) Substitutes a new tube reducing lubricant and thereafter complies with the requirements of paragraph (d)(3) of this section; or

(iii) Determines the source of the pollutant whose concentration exceeded the level specified in subparagraph (2) above and demonstrates to the satisfaction of the POTW control authority that such source has been eliminated.

(5) The concentration limits specified in paragraph (d)(2) of this section apply at the point of discharge from the tube reducing process. However, sampling after the tube reducing wastewater has been commingled with other wastewaters is permitted if:

(i) Any dilution caused by the other wastewaters is taken into account in determining the appropriate (i.e., lower) allowable discharge concentration; and

(ii) An analytical method of sufficient sensitivity is used to measure the levels of each of the foregoing nitrosamine compounds in the wastewaters being sampled.

(e) Drawing spent neat oils—subpart C—PSNS. There shall be no discharge of process wastewater pollutants.

(f) Drawing spent emulsions.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt drawn with emulsions Chromium0.0360.015 Nickel0.0530.036 Fluoride5.682.52

(g) Extrusion spent lubricants—subpart C—PSNS. There shall be no discharge of process wastewater pollutants.

(h) Extrusion press or solution heat treatment contact cooling water.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of extruded nickel-cobalt heat treated Chromium0.0310.013 Nickel0.0460.031 Fluoride4.952.20

(i) Extrusion press hydraulic fluid leakage.

Subpart C—NSPS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt extruded Chromium0.0860.034 Nickel0.1280.086 Fluoride13.86.13

(j) Forging equipment cleaning wastewater.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt forged Chromium0.0020.0006 Nickel0.0020.002 Fluoride0.2380.106

(k) Forging contact cooling water.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of forged nickel-cobalt cooled with water Chromium0.0180.007 Nickel0.0260.018 Fluoride2.821.25

(l) Forging press hydraulic fluid leakage.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt forged Chromium0.0690.028 Nickel0.1030.069 Fluoride11.24.94

(m) Forging spent lubricants—subpart C—PSNS. There shall be no discharge of process wastewater pollutants.

(n) Stationary casting contact cooling water.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt cast with stationary methods Chromium0.4480.182 Nickel0.6660.448 Fluoride72.032.0

(o) Vacuum melting steam condensate—subpart C—PSNS. There shall be no allowance for the discharge of process wastewater pollutants.

(p) Metal powder production atomization wastewater.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt metal powder atomized Chromium0.9700.393 Nickel1.440.970 Fluoride15669.2

(q) Annealing and Solution Heat Treatment Contact Cooling Water—subpart C—PSNS. There shall be no allowance for the discharge of process wastewater pollutant.

(r) Wet Air Pollution Control Scrubber Blowdown.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt formed Chromium0.3000.122 Nickel0.4500.300 Fluoride48.221.4

(s) Surface treatment spent baths.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt surface treated Chromium0.3460.141 Nickel0.5150.346 Fluoride55.724.7

(t) Surface treatment rinse.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt surface treated Chromium0.8740.354 Nickel1.300.873 Fluoride14162.3

(u) Alkaline cleaning spent baths.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt alkaline cleaned Chromium0.0130.005 Nickel0.0190.013 Fluoride2.020.895

(v) Alkaline cleaning rinse.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt alkaline cleaned Chromium0.0860.035 Nickel0.1280.086 Fluoride13.96.15

(w) Molten salt rinse.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt treated with molten salt Chromium0.3120.127 Nickel0.4640.312 Fluoride50.222.3

(x) Ammonia rinse.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt treated with ammonia solution Chromium0.0060.002 Nickel0.0080.006 Fluoride0.8810.391

(y) Sawing or grinding spent emulsions.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt sawed or ground with emulsions Chromium0.0150.006 Nickel0.0220.015 Fluoride2.351.04

(z) Sawing or grinding rinse.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of sawed or ground nickel-cobalt rinsed Chromium0.0670.027 Nickel0.1000.067 Fluoride10.84.78

(aa) Steam cleaning condensate.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt steam cleaned Chromium0.0110.005 Nickel0.0170.011 Fluoride1.790.795

(bb) Hydrostatic tube testing and ultrasonic testing wastewater—subpart C—PSNS. There shall be no allowance discharge of process wastewater pollutants.

(cc) Degreasing spent solvents—subpart C—PSNS. There shall be no discharge of process wastewater pollutants.

(dd) Dye penetrant testing wastewater.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt tested with dye penetrant method Chromium0.0790.032 Nickel0.1170.079 Fluoride12.75.63

(ee) Electrocoating rinse.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt electrocoated Chromium1.250.506 Nickel1.860.125 Fluoride20189.0

(ff) Miscellaneous wastewater sources.

Subpart C—PSNS

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average mg/off-kg (pounds per million off-pounds) of nickel-cobalt formed Chromium0.0910.037 Nickel0.1360.091 Fluoride14.76.50
[50 FR 34270, Aug. 23, 1985; 51 FR 2886, Jan. 22, 1986, as amended at 54 FR 11350, Mar. 17, 1989]

§ 471.36 - Effluent limitations representing the degree of effluent reduction attainable by the application of the best conventional pollutant control technology (BCT). [Reserved]